IDENTIFICATION AND DETERMINATION OF TRINITROTOLUENES IN WATER USING LIQUID CHROMATOGRAPHY TANDEM MASS SPECTROMETRY (LC-MS/MS)

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Authors

  • Khuat Hoang Binh (Corresponding Author) Institute of Chemistry and Materials, Academy of Military Science and Technology

Keywords:

Liquid mass chromatography method; Trinitrotoluene; Explosives.

Abstract

TNT is a highly toxic and potentially polluting explosive. Their trace content in water will be determined by LC-MS/MS using APCI ionization technique. The limit of detection of the method is 0,202 µg/l.

References

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[2]. A. Schmidt, B. Niehus, F. -M. Matysik,“Identification and Quantification of Polar Nitroaromatic Compounds in Explosive-Contaminated Waters by means of HPLC-ESI-MS-MS and HPLC-UV”, Chromatographia, 63 (1-2), pp. 1-11 (2006).

[3]. Becˇanova´, Friedl, Sˇimek, “Identification and determination of trinitrotoluenes and their degradation products using liquid chromatography- electrospray ionization mass spectrometry”, Int J Mass Spectrom, 291, pp. 133-139 (2010).

[4]. David DeTata, Peter Collins, Allan McKinley, “A fast liquid chromatography quadrupole time-of-flight mass spectrometry (LC-QToF-MS) method for the identification of organic explosives and propellants”, Forensic Science International, 233, pp. 63-74 (2013).

[5]. Din En Iso 22478, German Version EN ISO 22478, Beuth, Berlin (2006).

[6]. Method 8330, USEPA, SW-846, “Nitroaromatics, nitramines, and nitrat esters by hight performance liquid chromatography (HPLC)”, US Environmental Protection Agency, Washington, DC (1994).

Published

14-12-2020

How to Cite

Bình. “IDENTIFICATION AND DETERMINATION OF TRINITROTOLUENES IN WATER USING LIQUID CHROMATOGRAPHY TANDEM MASS SPECTROMETRY (LC-MS/MS)”. Journal of Military Science and Technology, no. 70, Dec. 2020, pp. 89-94, https://en.jmst.info/index.php/jmst/article/view/114.

Issue

Section

Research Articles