RESEARCH ON THE SYNTHESIS OF Ц-2 COMPOUND BY NON-SEPARATING TRANS-TAD METHOD
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Ц-2; Trans-TAD; TNAD; EDA.Abstract
In this paper, some results of research on synthesizing Trans-1,4,5,8-tetranitroso-1,4,5,8- tetraazadecalin (Ц-2) to use as an energy additive in propellant are presented. Research results show that when using reactants with mass ratio glyoxal/EDA/sodium nitrite/acetic acid/nitric acid 145/205/310/4,5/1890, the synthesis is carried out in two stages, the temperature of the first stage reaction is fixed at 55±2 oC, the second stage is fixed at 10±4 oC, and the time of the first stage is 5 o'clock, the nitric acid concentration is 30% gives the yield up to 71.18% and the product after synthesis and purification meets the requirements for use in preparing propellants used in artillery.
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